High Sensitivity Electrochemical As (III) Sensor Based on Fe3O4/MoS2 Nanocomposites

作者：Hu, Haibing^*; Hu, Yunhu; Xie, Baozhu; Zhu, Jianxiong^*

来源：Nanomaterials, 2023, 13(16): 2288.

DOI：10.3390/nano13162288

• As (III) detection
• electrochemical analysis method
• electrochemical sensors

Currently, heavy metal ion pollution in water is becoming more and more common, especially As (III), which is a serious threat to human health. In this experiment, a glassy carbon electrode modified with Fe3O4/MoS2 nanocomposites was used to select the square wave voltammetry (SWV) electrochemical detection method for the detection of trace As (III) in water. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) showed thatFe(3)O(4) nanoparticles were uniformly attached to the surface of MoS2 and were not easily agglomerated. Cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS) showed thatFe(3)O(4)/MoS2 has higher sensitivity and conductivity. After optimizing the experimental conditions, the Fe3O4/MoS2 -modified glassy carbon electrode exhibited high sensitivity (3.67 mu A/ppb) and a low detection limit (0.70 ppb), as well as excellent interference resistance and stability for As (III).